Table 5.
Spike concentration (µg/mL) | In sample (before addition) (µg/mL) | Expected (calculated) (µg/mL) | Actual (measured)(µg/mL) | Recovery (%) | RSD (%) |
---|---|---|---|---|---|
5 | 19.60 ± 0.24 | 24.60 | 24.57 ± 0.34 | 99.88 | 1.38 |
10 | 19.60 ± 0.24 | 29.60 | 29.48 ± 0.37 | 99.60 | 1.25 |
15 | 19.60 ± 0.24 | 34.60 | 34.50 ± 0.13 | 99.71 | 0.37 |