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. 2014 Feb 10;19(2):1887–1911. doi: 10.3390/molecules19021887

Table 1.

Extraction conditions of different methods used for L. chuanxiong rhizoma.

No. Constituents Method Solvent Time (min) Temperature (°C) Extraction yield (%) Ref.
1 Ferulic acid Ultrasound 4 mL ethanol 30 25 0.06 [9]
2 Ferulic acid Reflux 12 mL 75% ethanol 270 100 0.13 [10]
3 Ferulic acid Reflux 8 mL 70% ethanol 180 100 0.11 [11]
4 Ferulic acid Reflux 7.5 mL 80% ethanol 180 Unclear 0.11 [12]
5 Ferulic acid Percolation and decoction 12 mL water 180 100 0.05–0.06 [6]
6 Ferulic acid Reflux 6 mL 90% ethanol 358 Unclear 0.14 [13]
7 Ferulic acid Microwave 10 mL 40% ethanol 4 Unclear 0.08 [22]
8 Ferulic acid Reflux 54 mL 40% ethanol 180 100 0.10–0.19 [14]
9 Ferulic acid Reflux 5 mL 90% ethanol 90 100 0.11–0.18 [15]
10 Ferulic acid Reflux 5 mL water 60 50 0.05 [16]
11 Ferulic acid Reflux 8 mL 70% ethanol 180 100 0.11 [17]
12 Ferulic acid Ligustilide Reflux 15 mL 80% ethanol 180 Unclear 0.35–0.12;
0.07–0.20
[18]
13 Ligustilide Reflux 25 mL 71% ethanol 278 89 0.68 [19]
14 Senkyunolide A Ligustilide Distillation water 540 100 0.04;
0.21
[5]
15 Senkyunolide I Senkyunolide H Ligustilide Microwave 15 mL ionic liquid 5 180 about 0.08;
about 0.02;
about 0.40
[21]
16 Senkyunolide I Senkyunolide H Ligustilide Reflux 5 mL 75% ethanol 270 60 0.10–0.20;
0.05–0.09;
0.44–0.53
[20]
17 Ferulic acid Senkyunolide I Senkyunolide H Ligustilide Levistolide A Percolation and ultrasound 25 mL ethanol >300 Unclear 0.51;
1.32;
0.47;
3.74;
0.05
[7]

Note: 0.5 g sample to calculate the volume of extraction solvent.