Table 2.
Run order | X1 (°C) | X2 (W) | X3 (min) | Ferulic acid | Senkyunolide I | Senkyunolide H | Senkyunolide A | Ligustilide | Levistolide A |
---|---|---|---|---|---|---|---|---|---|
1 | 1(70) | 1(200) | 1(80) | 0.25 ± 0.01 | 0.09 ± 0.01 | 0.26 ± 0.01 | 0.70 ± 0.00 | 2.65 ± 0.01 | 0.04 ± 0.01 |
2 | 1(70) | 1(200) | −1(60) | 0.25 ± 0.01 | 0.09 ± 0.01 | 0.25 ± 0.03 | 0.69 ± 0.03 | 2.63 ± 0.01 | 0.04 ± 0.01 |
3 | 1(70) | −1(150) | 1(80) | 0.25 ± 0.01 | 0.09 ± 0.01 | 0.26 ± 0.01 | 0.67 ± 0.00 | 2.63 ± 0.01 | 0.04 ± 0.01 |
4 | 1(70) | −1(150) | −1(60) | 0.25 ± 0.01 | 0.08 ± 0.01 | 0.25 ± 0.01 | 0.64 ± 0.00 | 2.60 ± 0.01 | 0.04 ± 0.01 |
5 | −1(50) | 1(200) | 1(80) | 0.23 ± 0.01 | 0.09 ± 0.01 | 0.26 ± 0.02 | 0.69 ± 0.05 | 2.63 ± 0.01 | 0.04 ± 0.01 |
6 | −1(50) | 1(200) | −1(60) | 0.23 ± 0.01 | 0.09 ± 0.01 | 0.24 ± 0.01 | 0.68 ± 0.00 | 2.55 ± 0.01 | 0.04 ± 0.01 |
7 | −1(50) | −1(150) | 1(80) | 0.23 ± 0.01 | 0.06 ± 0.01 | 0.25 ± 0.01 | 0.67 ± 0.00 | 2.57 ± 0.01 | 0.04 ± 0.01 |
8 | −1(50) | −1(150) | −1(60) | 0.12 ± 0.01 | 0.05 ± 0.01 | 0.13 ± 0.01 | 0.42 ± 0.00 | 1.69 ± 0.01 | 0.02 ± 0.01 |
9 | −1.682(43) | 0(175) | 0(70) | 0.21 ± 0.01 | 0.05 ± 0.01 | 0.17 ± 0.07 | 0.52 ± 0.07 | 2.13 ± 0.01 | 0.03 ± 0.01 |
10 | 1.682(77) | 0(175) | 0(70) | 0.28 ± 0.01 | 0.10 ± 0.01 | 0.26 ± 0.04 | 0.67 ± 0.02 | 2.75 ± 0.01 | 0.05 ± 0.01 |
11 | 0(60) | −1.682(132.5) | 0(70) | 0.26 ± 0.01 | 0.08 ± 0.01 | 0.21 ± 0.01 | 0.63 ± 0.00 | 2.29 ± 0.01 | 0.03 ± 0.01 |
12 | 0(60) | 1.682(217.5) | 0(70) | 0.25 ± 0.01 | 0.09 ± 0.01 | 0.27 ± 0.01 | 0.79 ± 0.01 | 2.69 ± 0.01 | 0.04 ± 0.01 |
13 | 0(60) | 0(175) | −1.682(53) | 0.21 ± 0.01 | 0.08 ± 0.01 | 0.25 ± 0.01 | 0.58 ± 0.05 | 2.59 ± 0.01 | 0.04 ± 0.01 |
14 | 0(60) | 0(175) | 1.682(87) | 0.25 ± 0.01 | 0.09 ± 0.01 | 0.27 ± 0.01 | 0.74 ± 0.00 | 2.82 ± 0.01 | 0.04 ± 0.01 |
15 | 0(60) | 0(175) | 0(70) | 0.24 ± 0.01 | 0.08 ± 0.01 | 0.24 ± 0.01 | 0.64 ± 0.00 | 2.60 ± 0.01 | 0.04 ± 0.01 |
16 | 0(60) | 0(175) | 0(70) | 0.25 ± 0.01 | 0.09 ± 0.01 | 0.25 ± 0.02 | 0.66 ± 0.06 | 2.72 ± 0.01 | 0.04 ± 0.01 |
17 | 0(60) | 0(175) | 0(70) | 0.23 ± 0.01 | 0.09 ± 0.01 | 0.26 ± 0.01 | 0.66 ± 0.00 | 2.57 ± 0.01 | 0.04 ± 0.01 |
18 | 0(60) | 0(175) | 0(70) | 0.24 ± 0.01 | 0.09 ± 0.01 | 0.27 ± 0.01 | 0.68 ± 0.00 | 2.66 ± 0.01 | 0.04 ± 0.01 |
19 | 0(60) | 0(175) | 0(70) | 0.26 ± 0.01 | 0.09 ± 0.01 | 0.29 ± 0.03 | 0.67 ± 0.03 | 2.75 ± 0.01 | 0.04 ± 0.01 |
20 | 0(60) | 0(175) | 0(70) | 0.24 ± 0.01 | 0.09 ± 0.01 | 0.24 ± 0.08 | 0.63 ± 0.03 | 2.71 ± 0.01 | 0.04 ± 0.01 |