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. 2014 Feb 6;19(2):1820–1827. doi: 10.3390/molecules19021820

Table 1.

1H- and 13C- NMR Data of compounds 1 and 2 at 400 and 100 MHz, resp., in acetone-d6. δ in ppm, J in Hz.

Position 1 2
δH δC δH δC
1 161.9 165.9
2 111.1 111.8
3 163.7 170.3
4 6.42 s 93.3 105.0
4a 156.3 158.3
5 7.23 d (9.2) 116.8 7.70 d (8.0) 115.9
5a 152.4 145.7
6 7.33 d (9.2) 124.5 7.37 dd (8.0, 7.6) 126.2
7 152.5 7.44 d (7.6) 121.9
8 131.1 147.4
8a 119.6 122.1
9 184.3 181.9
9a 104.3 103.0
10 3.37 d (7.2) 22.1 3.36 d (7.2) 21.6
11 5.29 t (7.2) 123.6 5.26 t (7.2) 122.3
12 131.6 132.5
13 1.79 s 18.1 1.80 s 18.0
14 1.65 s 26.0 1.66 s 25.9
15 3.49 t (7.6) 22.6 206.1
16 1.84 t (7.6) 44.5 3.67 s 55.3
17 71.1 72.0
18 1.30 s 29.8 1.45 s 30.4
19 1.30 s 29.8 1.45 s 30.4
OH-1 13.69 s 14.33 s a
OH-3 9.68 s 14.40 s a
OH-7 8.72 s
OH-8 15.12 s a
OH-18 3.81 s 2.81 s

a These data may be interchanged.