Table 1.
Position | 1 | 2 | |||
---|---|---|---|---|---|
δH | δC | δH | δC | ||
1 | 161.9 | 165.9 | |||
2 | 111.1 | 111.8 | |||
3 | 163.7 | 170.3 | |||
4 | 6.42 s | 93.3 | 105.0 | ||
4a | 156.3 | 158.3 | |||
5 | 7.23 d (9.2) | 116.8 | 7.70 d (8.0) | 115.9 | |
5a | 152.4 | 145.7 | |||
6 | 7.33 d (9.2) | 124.5 | 7.37 dd (8.0, 7.6) | 126.2 | |
7 | 152.5 | 7.44 d (7.6) | 121.9 | ||
8 | 131.1 | 147.4 | |||
8a | 119.6 | 122.1 | |||
9 | 184.3 | 181.9 | |||
9a | 104.3 | 103.0 | |||
10 | 3.37 d (7.2) | 22.1 | 3.36 d (7.2) | 21.6 | |
11 | 5.29 t (7.2) | 123.6 | 5.26 t (7.2) | 122.3 | |
12 | 131.6 | 132.5 | |||
13 | 1.79 s | 18.1 | 1.80 s | 18.0 | |
14 | 1.65 s | 26.0 | 1.66 s | 25.9 | |
15 | 3.49 t (7.6) | 22.6 | 206.1 | ||
16 | 1.84 t (7.6) | 44.5 | 3.67 s | 55.3 | |
17 | 71.1 | 72.0 | |||
18 | 1.30 s | 29.8 | 1.45 s | 30.4 | |
19 | 1.30 s | 29.8 | 1.45 s | 30.4 | |
OH-1 | 13.69 s | 14.33 s a | |||
OH-3 | 9.68 s | 14.40 s a | |||
OH-7 | 8.72 s | ||||
OH-8 | 15.12 s a | ||||
OH-18 | 3.81 s | 2.81 s |
a These data may be interchanged.