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. 2014 Sep 29;19(10):15754–15767. doi: 10.3390/molecules191015754

Scheme 4.

Synthesis of bis(ara-F NMN) (20), bis(ara-F NMN)[CH2] (21) and bis(2′-CH3- 2′-F NMN)[CH2] (22).

Scheme 4

Reagents and conditions: (a) CDI, DMF, MeOH, rt, 3 days; (b) TMP, methylenebis(phosphonic dichloride), 0 °C, 5 h.