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. 2015 Mar 20;20(3):5165–5183. doi: 10.3390/molecules20035165

Table 3.

DLS results of PPI, SSPS, and complex emulsions before and after long-term storage in pH 6 with 0.2 M NaCl at 4 °C.

Sample SDS Concentration after Dilution (%) a Dh (nm) PDI
SSPS fresh 0 724 ± 12 0.62 ± 0.08
after 2 weeks 0 752 ± 23 1.0
0.3 699 ± 17 0.27 ± 0.09
PPI1 cannot produce homogeneous emulsion
PPI2 fresh 0 1094 ± 21 0.26 ± 0.05
after 1 weeks 0 9025 ± 1008 1.0
0.3 798 ± 17 0.77 ± 0.04
PPI3 fresh 0 1138 ± 15 0.13 ± 0.05
after 2 weeks 0 8774 ± 198 1.0
0.3 736 ± 28 0.81 ± 0.02
PPI4 cannot produce homogeneous emulsion
Complex1 fresh 0 319 ± 8 0.27 ± 0.09
after12 months 0 426 ± 26 0.14 ± 0.10
0.3 371 ± 20 0.16 ± 0.03
Complex2 fresh 0 283 ± 7 0.16 ± 0.05
after 14 months 0 331 ± 24 0.12 ± 0.02
0.3 312 ± 12 0.16 ± 0.02
Complex3 fresh 0 325 ± 6 0.23 ± 0.06
after 12 months 0 421 ± 28 0.25 ± 0.10
0.3 388 ± 2 0.24 ± 0.13
Complex3 (unheated) fresh 0 740 ± 70 0.74 ± 0.26
after 12 months 0 3374 ± 245 1.0
0.3 404 ± 50 0.60 ± 0.17
Complex4 fresh 0 328 ± 27 0.20 ± 0.03
after 11 months 0 482 ± 178 0.31 ± 0.14
0.3 404 ± 118 0.22 ± 0.09

a The DLS samples were prepared by diluting 5 μL of the creaming layer with 3 mL of solution containing the same pH and NaCl concentration as well as 0 or 0.3% SDS.