Table 2.
No. | 1 a | 2 b | 3 a | 4 b | 5 a | 6 c | 7 d |
---|---|---|---|---|---|---|---|
1 | 38.9 t | 40.0 t | 38.9 t | 40.0 t | 38.7 t | 39.5 t | 30.7 t |
2 | 24.3 t | 25.3 t | 24.2 t | 25.1 t | 25.3 t | 25.0 t | 24.7 t |
3 | 78.9 d | 80.7 t | 79.0 d | 80.8 t | 79.0 d | 79.5 d | 79.9 d |
4 | 48.0 s | 48.8 s | 48.1 s | 49.0 s | 47.8 s | 49.6 s | 48.3 s |
5 | 56.4 d | 57.3 d | 56.4 d | 57.3 d | 56.3 d | 46.0 d | 49.6 d |
6 | 21.9 t | 23.0 t | 22.0 t | 23.0 t | 21.4 t | 18.9 t | 21.5 t |
7 | 41.9 t | 43.0 t | 41.9 t | 43.0 t | 40.9 t | 38.1 t | 34.8 t |
8 | 45.2 s | 45.5 s | 45.2 s | 45.5 s | 43.8 s | 42.3 s | 54.2 s |
9 | 56.1 d | 57.3 d | 56.0 d | 57.3 d | 55.1 d | 155.6 s | 75.6 s |
10 | 39.5 s | 40.5 s | 39.5 s | 40.5 s | 39.3 s | 38.4 s | 44.4 s |
11 | 18.5 t | 19.7 t | 18.5 t | 19.7 t | 18.5 t | 115.2 t | 26.6 t |
12 | 26.9 t | 27.2 t | 26.9 t | 27.2 t | 33.0 t | 38.0 t | 31.5 t |
13 | 49.0 d | 46.2 d | 48.9 d | 46.2 d | 43.7 d | 41.2 d | 41.1 d |
14 | 37.6 t | 38.0 t | 37.5 t | 38.0 t | 39.4 t | 44.9 t | 45.1 t |
15 | 57.5 t | 53.5 t | 57.5 t | 53.5 t | 48.7 t | 51.0 d | 134.2 d |
16 | 79.6 s | 82.8 s | 79.7 s | 82.8 s | 155.0 s | 158.2 s | 149.2 s |
17 | 24.1 q | 66.8 t | 24.1 q | 66.8 t | 103.0 t | 106.0 t | 60.9 t |
18 | 24.7 q | 24.5 q | 24.7 q | 24.5 q | 23.6 q | 24.3 q | 24.4 q |
19 | 178.1 s | 177.9 s | 178.3 s | 178.1 s | 180.0 s | 178.1 s | 176.0 s |
20 | 15.7 q | 16.1 q | 15.7 q | 16.1 q | 15.3 q | 23.3 q | 17.4 q |
3-ester | 167.9 s | 169.4 s | 167.9 s | 169.4 s | 173.0 s | 166.8 s | 166.9 s |
128.1 s | 129.3 s | 128.9 s | 129.5 s | 36.0 t | 118.4 d | 119.5 d | |
138.6 d | 139.0 d | 137.8 d | 138.8 d | 30.9 t | 145.3 d | 145.2 d | |
16.0 q | 16.0 q | 14.7 q | 14.4 q | 140.0 s | 134.5 s | 135.4 s | |
20.9 q | 20.9 q | 12.3 q | 12.1 q | 128.0 d | 128.4 d | 129.0 d | |
128.0 d | 129.1 d | 131.1 d | |||||
126.0 d | 130.5 d | 129.8 d |
a Recorded in CDCl3 at 100 MHz; b Recorded in CD3OD at 100 MHz; c Recorded in CDCl3 at 150 MHz; d Recorded in acetone-d6 at 100 MHz.