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. 2016 Aug 19;21(8):1089. doi: 10.3390/molecules21081089

Table 2.

13C-NMR Data of compounds 13.

Carbon 1 a 2 b 3 b
1 111.3 111.0 112.3
2 153.3 153.5 156.0
3 99.7 99.7 c 117.7
4 157.9 157.9 158.6
5 128.8 128.8 129.6
6 116.6 116.6 114.4
7 154.1 154.1 156.8
8 110.9 110.9 115.4
9 126.7 126.8 31.8
10 125.0 124.7 31.4
4a 114.2 114.2 121.1
4b 123.6 123.6 126.3
8a 132.5 132.4 140.9
10a 133.4 133.3 141.9
1′ 110.6 111.0 110.9
2′ 153.1 153.3 154.3
3′ 99.0 99.8 c 100.5
4′ 157.7 157.8 160.5
5′ 112.7 123.5 130.5
6′ 145.6 117.4 117.2
7′ 144.2 145.5 158.1
8′ 111.7 140.8 109.5
9′ 126.5 120.0 128.6
10′ 121.5 124.7 126.5
4a′ 113.8 114.2 116.7
4b′ 124.4 124.3 126.6
8a′ 125.6 126.2 134.5
10a′ 133.8 133.4 135.2
4-OCH3 55.5 55.5 60.0
4′-OCH3 55.5 55.5 56.2
7′-OCH3 55.8
8′-OCH3 60.3

a 13C-NMR data were measured at 150 MHZ in DMSO-d6 for 1, δ in ppm; b 13C-NMR data were measured at 125 MHZ in DMSO-d6 for 2, in CD3OD for 3, δ in ppm, J in Hz; c the signals under the same superscript may be interchanged.