Figure 12.
Preparation of diastereomeric amides 16a and 16b (a), separation by HPLC on silica gel (b), and preparation of methyl ester (S)-(−)-17 (c). HPLC, redrawn from [24].
Preparation of diastereomeric amides 16a and 16b (a), separation by HPLC on silica gel (b), and preparation of methyl ester (S)-(−)-17 (c). HPLC, redrawn from [24].