Table 1.
Complex | Step | Thermal Effect | Temperature Range (°C) | Δmexp (%) | Δmcalc (%) |
---|---|---|---|---|---|
(1) | 1 | Exothermic | 320–1000 | 72.5 | 72.8 |
Residue (Sm2O3) | 27.5 | 27.2 | |||
(2) | 1 | Endothermic | 170–300 | 5.0 | 5.3 |
2 | Exothermic | 320–1000 | 72.2 | 72.3 | |
Residue (Eu2O3) | 22.8 | 22.4 | |||
(3) | 1 | Endothermic | 240–315 | 2.6 | 2.7 |
2 | Exothermic | 325–1000 | 69.9 | 70.1 | |
Residue (Gd2O3) | 27.5 | 27.2 | |||
(4) | 1 | Endothermic | 210–310 | 2.5 | 2.7 |
2 | Exothermic | 320–1000 | 69.6 | 69.9 | |
Residue (Tb2O3) | 27.9 | 27.4 |