. 2016 Nov 4;21(11):1475. doi: 10.3390/molecules21111475

Table 1.

Calibration data of four analytes.

Analyte ^a	Linear Range (μg·mL⁻¹)	Calibration Equation ^b	r²	LOD (μg·mL⁻¹)	LOQ (μg·mL⁻¹)	Intra-Day RSD (%) (n = 6)			Inter-Day RSD (%) (n = 6)			Recovery and RSD (%) (Mean, n = 6)
Analyte ^a	Linear Range (μg·mL⁻¹)	Calibration Equation ^b	r²	LOD (μg·mL⁻¹)	LOQ (μg·mL⁻¹)	L1	L3	L5	L1	L3	L5	Recovery and RSD (%) (Mean, n = 6)
1	3.1~32.2	Y = 7701.546x + 9983	0.9992	0.26	0.81	2.46	1.91	1.36	1.06	0.98	1.39	105.54, 3.32
2	3.1~32.2	Y = 5548.525x + 15,762	0.9995	0.29	0.95	3.27	2.38	1.57	1.62	1.78	1.20	104.06, 2.96
3	20.5~520.6	Y = 7171.274x + 31,544	0.9993	0.03	0.11	3.36	1.50	2.02	1.83	1.19	1.14	102.95, 3.37
4	3.1~32.2	Y = 9108.011x + 6141	0.9996	0.11	0.37	2.50	1.66	1.46	1.79	1.54	1.44	104.92, 2.70

^a The compound codes 1, 2, 3, and 4 of each analyte refers to epimedin A, epimedin B, epimedin C, and icariin, respectively; ^b Y: peak area; X: concentration of compound (μg·mL⁻¹).