Umbilicaxanthone A (CDCl3) | ||
---|---|---|
Position | δC | δH (J in Hz) |
1 | 150.9 | - |
1–OH | - | 13.25 (s) (1H) |
2 | 118.2 | - |
3 | 120.1 | 6.51 (s) (1H) |
4 | 142.6 | - |
4–OCH3 | 56.4 | 3.75 (s) (3H) |
4a | 140.9 | - |
5 | 146.4 | - |
6 | 102.1 | 6.15 (d, 2.1) (1H) |
7 | 156.9 | - |
8 | 106.3 | a |
8a | 128.9 | - |
9 | 179.8 | - |
9a | 116.1 | - |
10a | 136.5 | - |
1′ | 22.0 | 3.19 (d, 6.6) (2H) |
2′ | 123.5 | 5.92 (td, 6.6, 1.3) (1H) |
3′ | 131.3 | - |
4′ | 25.9 | 1.64 (s) (3H) |
5′ | 17.9 | 1.57 (s) (3H) |