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. 2016 Mar 2;21(3):294. doi: 10.3390/molecules21030294
Linolenoylumbilicaxanthoside B (CDCl3)
Position δC δH (J in Hz)
1 151.0 -
1–OH - 13.30 (s) (1H)
2 117.8 -
3 119.4 6.47 (s) (1H)
4 143.2 -
4–OCH3 56.3 3.75 (s) (3H)
4a 141.3 -
5 147.1 -
6 103.7 6.42 (s) (1H)
7 153.2 -
8 118.4 -
8a 129.6 -
9 183.1 -
9a 114.6 -
10a 135.7 -
1′ 25.4 3.38 (d, 7.2) (2H)
2′ 123.8 5.39 (dd, 7.2, 1.2) (1H)
3′ 130.9 -
4′ 26.2 1.65 (s) (3H)
5′ 18.4 1.79 (s) (3H)
1″ 26.1 4.19 (d, 6.8) (2H)
2″ 124.8 5.37 (dd, 6.8, 1.5) (1H)
3″ 132.0 -
4″ 25.9 1.67 (s) (3H)
5″ 18.0 1.84 (s) (3H)
1‴ 99.8 5.05 (d, 8.1) (1H)
2‴ 74.2 3.50 (dd, 8.9, 8.1) (1H)
3‴ 77.1 3.58 (t, 8.9) (1H)
4‴ 76.7 3.05 (dd, 9.3, 8.9) (1H)
5‴ 76.1 3.54 (m) (1H)
6‴ 65.3 4.51 (dd, 12.1, 2.3) (1H)
4.03 (dd, 12.1, 5.2) (1H)
1’’’’ 104.1 5.15 (d, 8.0) (1H)
2’’’’ 73.8 3.52 (dd, 9.0, 8.0) (1H)
3’’’’ 76.5 3.61 (t, 9.0) (1H)
4’’’’ 69.7 3.41 (t, 9.0) (1H)
5’’’’ 76.9 3.45 (m) (1H)
6’’’’ 62.6 3.93 (dd, 12.1, 2.2) (1H)
3.72 (dd, 12.1, 5.2) (1H)
1’’’’’ 172.0 -
2’’’’’ 34.6 2.25 (m) (2H)
3’’’’’ 25.0 1.68 (m) (2H)
4’’’’' 29.2 1.29 (m) (6H)
5’’’’’ 29.3 1.29 (m) (6H)
6’’’’’ 29.1 1.29 (m) (6H)
7’’’’’ 30.3 1.33 (m) (2H)
8’’’’’ 27.3 1.96 (m) (2H)
9’’’’’ 131.8 5.37 (m) (1H)
10’’’’’ 131.7 5.42 (m) (1H)
11’’’’’ 25.7 2.68 (m) (2H)
12’’’’’ 128.3 5.35 (m) (2H)
13’’’’’ 128.4 5.35 (m) (2H)
14’’’’’ 25.6 2.73 (m) (2H)
15’’’’’ 127.1 5.43 (m) (1H)
16’’’’’ 131.9 5.36 (m) (1H)
17’’’’’ 20.6 1.93 (m) (2H)
18’’’’’ 14.2 1.06 (t, 6.8) (3H)