Secalonic Acid A (CDCl3) | ||
---|---|---|
Position | δC | δH (J in Hz) |
1, 1′ | 159.4 | - |
–OH 1,1′ | - | 11.75 (s) (2H) |
2, 2′ | 118.2 | - |
3, 3′ | 140.2 | 7.46 (d, 8.5) (2H) |
4, 4′ | 107.6 | 6.63 (d, 8.5) (2H) |
4a, 4a′ | 158.3 | - |
5, 5′ | 76.9 | 3.93 (dd, 11.3, 1.6) (2H) |
–OH 5,5′ | - | 2.81 (d, 2.2) (2H) |
6, 6′ | 29.2 | 2.41 (m) (2H) |
7, 7′ | 36.3 | 2.74 (dd, 19.0, 6.1) (2H) |
2.32 (dd, 19.0, 11.5) (2H) | ||
8, 8′ | 177.5 | - |
–OH 8,8′ | - | 13.78 (s) (2H) |
8a, 8a′ | 101.5 | - |
9, 9′ | 187.2 | - |
9a, 9a′ | 106.9 | - |
10a, 10a′ | 84.7 | - |
11, 11′ | 18.0 | 1.17 (d, 6.4) (6H) |
12, 12′ | 170.3 | - |
13, 13′ | 53.3 | 3.73 (s) (6H) |