Secalonic acid B (CDCl3) | ||
---|---|---|
Position | δC | δH (J in Hz) |
1, 1′ | 159.4 | - |
–OH 1,1′ | - | 11.85 (s) (2H) |
2, 2′ | 118.7 | - |
3, 3′ | 139.7 | 7.42 (d, 8.5) (2H) |
4, 4′ | 107.5 | 6.57 (d, 8.5) (2H) |
4a, 4a′ | 157.2 | - |
5, 5′ | 71.4 | 4.12 (d, 1.4) (2H) |
–OH 5,5′ | - | 2.57 (s) (2H) |
6, 6′ | 28.5 | 2.12 (m) (2H) |
7, 7′ | 32.6 | 7, 7′ α 2.52 (dd, 19.0, 11.5) (2H) |
7, 7′ β 2.41 (dd, 19.0, 6.1) (2H) | ||
8, 8′ | 179.8 | - |
–OH 8,8′ | - | 13.96 (s) (2H) |
8a, 8a′ | 99.9 | - |
9, 9′ | 187.7 | - |
9a, 9a′ | 107.0 | - |
10a, 10a′ | 84.8 | - |
11, 11′ | 17.5 | 1.18 (d, 6.8) (6H) |
12, 12′ | 171.2 | - |
13, 13′ | 53.4 | 3.72 (s) (6H) |