Table 1.
Compound | R | m.p. (°C) | Yields (%) a |
---|---|---|---|
5 | 171–173 | 51 | |
6 | 171–173 | 57 | |
7 | 185–186 | 68 | |
8 | 174–176 | 83 | |
9 | 176–178 | 81 | |
10 | 179–181 | 83 | |
11 | 186–188 | 79 | |
12 | 180–182 | 76 | |
13 | 178–180 | 82 | |
14 | 187–189 | 81 | |
15 | 156–158 | 91 | |
16 | 161–163 | 86 | |
17 | 188–190 | 82 | |
18 | 202–204 | 70 | |
19 | 192–193 | 84 | |
20 | 194–196 | 75 | |
21 | 198–200 | 83 | |
22 | 181–183 | 85 | |
23 | 204–206 | 77 | |
24 | 184–186 | 82 | |
25 | 135–137 | 86 |
a Yields represent isolated yields.