Table 2.
Crystallographic data for 3.
| Complex 3 | |
|---|---|
| Empirical formula | C14H18AgN3O7 |
| Formula weight | 448.18 |
| Crystal system | Monoclinic |
| Space group | P21/c |
| a (Å) | 9.7304(1) |
| b (Å) | 14.7348(2) |
| c (Å) | 14.0158(2) |
| α (°) | 90.000 |
| β (°) | 127.803(1) |
| γ (°) | 90.000 |
| V (Å3) | 1587.77(4) |
| Z | 4 |
| T (K) | 100(2) |
| F(000) | 904 |
| Dx (g·cm−3) | 1.875 |
| μ (mm−1) | 1.32 |
| Scan method | ω scan |
| θ range (°) | 2.3–28.0 |
| Measured reflections | 27856 |
| Unique reflections | 3836 |
| Observed reflections [I > 2σ(I)] | 3729 |
| Completeness to θmax (%) | 100 |
| No. of parameters/restraints | 271/18 |
| R [I > 2σ(I)] | 0.0147 |
| wR (all data) | 0.0379 |
| S | 1.09 |
| Largest diff. peak (e·Å−3) | 0.48 |
| Largest diff. hole (e·Å−3) | −0.30 |