Table 2.
Sample | CRS/TRS | |||
---|---|---|---|---|
Attribution | γ | β | α | α c |
E′/MPa | 18.33/7.48 | 26.28/11.71 | 40.20/23.54 | 38.34/25.73 |
Tan δ | 10.45/7.21 | 6.24/4.72 | 23.49/19.36 | N/A |
TE′/°C | 41.64/43.28 | 96.12/109.07 | 235.34/238.48 | 269.92/272.39 |
Ttanδ/°C | 39.91/42.11 | 92.72/100.55 | 214.25/218.92 | N/A |
ΔTE′/°C | 2.18 | 12.95 | 3.14 | 2.47 |
ΔTtanδ/°C | 2.20 | 7.83 | 4.67 | N/A |
* E′ and tan δ represent the storage modulus and integral loss factor of CRS and TRS samples at 1 Hz frequency respectively in DMA tensile mode. TE′ and Ttanδ represent the peak temperatures for the storage modulus and the loss factor curves, which are corresponding to the protein relaxation of γ, β, α and αc. ΔTE′ and ΔTtanδ represent the peak temperature differences between TRS and CRS samples at γ, β, or α-relaxation regions. The E′ and Tan δ values have an error bar of ±0.3, the TE′ and Ttanδ values have an error bar of ±0.5 °C.