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. Author manuscript; available in PMC: 2018 Dec 3.
Published in final edited form as: J Am Chem Soc. 2018 Nov 15;140(47):16184–16189. doi: 10.1021/jacs.8b09120

Figure 3.

Figure 3.

1H NMR spectra (C6D6, 500 MHz): (top) Ti8 with Ar2O standard; (middle): after 15 min of irradiation with excess benzhydrol; (bottom) after addition of tBu3ArO•. Peaks marked with purple # correspond to Ti8, while orange # correspond to the speculative H atom reduced cluster.