Table 1.
Position | Dasycladin A (1) in D2O | HMBC C |
Dasycladin B (2) in D2O | HMBC C |
||
---|---|---|---|---|---|---|
δH | δC, Type | δH | δC, Type | |||
2 | 163.3, C | 161.0, C | ||||
3 | 136.1, C | 134.1, C | ||||
4 | 7.40 (s) | 134.4, CH | 2, 3, 5, 9 | 7.94 (s) | 133.3, CH | 2, 3, 5, 9 |
5 | 118.3, C | 7.64 (s) | 122.4, CH | 4, 6, 7, 9 | ||
6 | 144.1, C | 137.6, C | ||||
7 | 152.7, C | 153.0, C | ||||
8 | 7.10 (s) | 106.8, CH | 6, 7, 9, 10 | 7.05 (s) | 105.1, CH | 6, 7, 9, 10 |
9 | 150.2, C | 151.1, C | ||||
10 | 113.5, C | 112.1, C | ||||
2′ | 163.0, C | |||||
3′ | 135.8, C | |||||
4′ | 7.96 (s) | 135.8, CH | 2′, 3′, 5′, 9′ | |||
5′ | 7.28 (s) | 115.8, CH | 4′, 6′, 7′, 9′ | |||
6′ | 145.7, C | |||||
7′ | 151.5, C | |||||
8′ | 111.2, C | |||||
9′ | 147.7, C | |||||
10′ | 113.9, C |