| Crystal data |
| Chemical formula |
(C10H8S8)2[Cu(CNS)4]·2C10H8S8
|
|
M
r
|
1834.43 |
| Crystal system, space group |
Monoclinic, P21/c
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
16.9036 (17), 21.004 (2), 9.6205 (9) |
| β (°) |
103.071 (3) |
|
V (Å3) |
3327.1 (6) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
1.50 |
| Crystal size (mm) |
0.18 × 0.16 × 0.02 |
| |
| Data collection |
| Diffractometer |
Bruker Kappa APEXII Quazar CCD |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2012 ▸) |
|
T
min, T
max
|
0.652, 0.745 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
48335, 5028, 3816 |
|
R
int
|
0.070 |
| θmax (°) |
23.7 |
| (sin θ/λ)max (Å−1) |
0.566 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.032, 0.078, 1.02 |
| No. of reflections |
5028 |
| No. of parameters |
385 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.38, −0.39 |
