Refinement on F2
|
Hydrogen site location: inferred from neighbouring sites |
Least-squares matrix: full |
H-atom parameters constrained |
R[F2 > 2σ(F2)] = 0.051 |
w = 1/[σ2(Fo2) + (0.0347P)2 + 0.7348P] where P = (Fo2 + 2Fc2)/3 |
wR(F2) = 0.122 |
(Δ/σ)max < 0.001 |
S = 1.10 |
Δρmax = 0.21 e Å−3
|
2589 reflections |
Δρmin = −0.20 e Å−3
|
195 parameters |
Extinction correction: SHELXL-2016/4 (Sheldrick 2016), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4
|
0 restraints |
Extinction coefficient: 0.0035 (12) |
Primary atom site location: dual |
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