| Crystal data |
| Chemical formula |
[Al2La2(CH3)6(C20H15O2)4(CH3O)2]·4C7H8
|
|
M
r
|
2001.86 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
13.8404 (6), 14.2089 (6), 14.6084 (7) |
| α, β, γ (°) |
73.198 (1), 81.968 (1), 63.523 (1) |
|
V (Å3) |
2461.54 (19) |
|
Z
|
1 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.93 |
| Crystal size (mm) |
0.43 × 0.17 × 0.14 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII CCD |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2008 ▸) |
|
T
min, T
max
|
0.713, 0.848 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
30779, 13082, 10174 |
|
R
int
|
0.065 |
| (sin θ/λ)max (Å−1) |
0.682 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.049, 0.111, 1.01 |
| No. of reflections |
13082 |
| No. of parameters |
596 |
| No. of restraints |
2 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.25, −1.36 |
