| Crystal data |
| Chemical formula |
C16H19N5O |
|
M
r
|
297.36 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
150 |
|
a, b, c (Å) |
5.3265 (2), 9.9946 (4), 14.5414 (5) |
| α, β, γ (°) |
103.054 (2), 100.039 (2), 93.108 (2) |
|
V (Å3) |
739.03 (5) |
|
Z
|
2 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
0.71 |
| Crystal size (mm) |
0.25 × 0.21 × 0.02 |
| |
| Data collection |
| Diffractometer |
Bruker D8 VENTURE PHOTON 100 CMOS |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
T
min, T
max
|
0.84, 0.97 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
5735, 2764, 2281 |
|
R
int
|
0.030 |
| (sin θ/λ)max (Å−1) |
0.617 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.041, 0.100, 1.07 |
| No. of reflections |
2764 |
| No. of parameters |
276 |
| H-atom treatment |
All H-atom parameters refined |
| Δρmax, Δρmin (e Å−3) |
0.25, −0.21 |
