Bruker SMART CCD area detector diffractometer | 3728 independent reflections |
Radiation source: fine-focus sealed tube | 3475 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.015 |
phi and ω scans | θmax = 28.1°, θmin = 1.7° |
Absorption correction: multi-scan (SADABS; Bruker, 2013) | h = −9→9 |
Tmin = 0.815, Tmax = 0.989 | k = −12→12 |
9076 measured reflections | l = −15→15 |