| Crystal data |
| Chemical formula |
C19H23N3O |
C19H24N4
|
|
M
r
|
309.40 |
308.42 |
| Crystal system, space group |
Monoclinic, P21/c
|
Monoclinic, C2/c
|
| Temperature (K) |
296 |
296 |
|
a, b, c (Å) |
9.2357 (7), 15.6388 (12), 11.984 (1) |
34.9185 (14), 8.4656 (5), 11.8361 (6) |
| β (°) |
93.998 (3) |
91.061 (5) |
|
V (Å3) |
1726.7 (2) |
3498.2 (3) |
|
Z
|
4 |
8 |
| Radiation type |
Mo Kα |
Mo Kα |
| μ (mm−1) |
0.08 |
0.07 |
| Crystal size (mm) |
0.15 × 0.15 × 0.10 |
0.15 × 0.10 × 0.10 |
| |
| Data collection |
| Diffractometer |
Bruker Kappa APEXII CCD |
Bruker Kappa APEXII CCD |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2016 ▸) |
Multi-scan (SADABS; Bruker, 2016 ▸) |
|
T
min, T
max
|
0.552, 0.746 |
0.697, 0.745 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
16458, 3208, 2109 |
32313, 3259, 1834 |
|
R
int
|
0.044 |
0.071 |
| (sin θ/λ)max (Å−1) |
0.606 |
0.606 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.047, 0.119, 1.03 |
0.049, 0.159, 1.02 |
| No. of reflections |
3208 |
3259 |
| No. of parameters |
218 |
218 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.15, −0.13 |
0.22, −0.18 |
