Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C22H28ClNO |
| M r | 357.90 |
| Crystal system, space group | Monoclinic, P21/m |
| Temperature (K) | 296 |
| a, b, c (Å) | 9.6753 (10), 7.0072 (6), 15.3749 (13) |
| β (°) | 93.425 (7) |
| V (Å3) | 1040.51 (17) |
| Z | 2 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.19 |
| Crystal size (mm) | 0.74 × 0.65 × 0.48 |
| Data collection | |
| Diffractometer | Stoe IPDS 2 |
| Absorption correction | Integration (X-RED32; Stoe & Cie, 2002 ▸) |
| T min, T max | 0.879, 0.940 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 5895, 2300, 1298 |
| R int | 0.028 |
| (sin θ/λ)max (Å−1) | 0.628 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.053, 0.168, 1.00 |
| No. of reflections | 2300 |
| No. of parameters | 145 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.28, −0.22 |