| Crystal data |
| Chemical formula |
4C18H15OP·2C14H10O4S |
|
M
r
|
1661.64 |
| Crystal system, space group |
Monoclinic, P21/c
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
10.7085 (1), 41.9751 (2), 18.9268 (1) |
| β (°) |
101.490 (1) |
|
V (Å3) |
8336.92 (10) |
|
Z
|
4 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
1.83 |
| Crystal size (mm) |
0.17 × 0.16 × 0.09 |
| |
| Data collection |
| Diffractometer |
XtaLAB Synergy, Dualflex, AtlasS2 |
| Absorption correction |
Gaussian (CrysAlis PRO; Rigaku OD, 2018 ▸) |
|
T
min, T
max
|
0.653, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
94929, 17036, 15740 |
|
R
int
|
0.025 |
| (sin θ/λ)max (Å−1) |
0.630 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.033, 0.092, 1.04 |
| No. of reflections |
17036 |
| No. of parameters |
1079 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.42, −0.55 |
