| Rigaku R-AXIS RAPIDII diffractometer | 3040 reflections with I > 2σ(I) |
| Detector resolution: 10.000 pixels mm-1 | Rint = 0.057 |
| ω scans | θmax = 30.0°, θmin = 3.0° |
| Absorption correction: numerical (NUMABS; Higashi, 1999) | h = −7→7 |
| Tmin = 0.716, Tmax = 0.873 | k = −20→19 |
| 21546 measured reflections | l = −21→22 |
| 3266 independent reflections |
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