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. 2018 Nov 6;74(Pt 12):1710–1716. doi: 10.1107/S2056989018015207
Oxford Diffraction Xcalibur single crystal X-ray diffractometer with Sapphire CCD detector 2178 reflections with I > 2σ(I)
Radiation source: Enhance (Mo) X-ray Source Rint = 0.021
Rotation method data acquisition using ω scans. θmax = 25.4°, θmin = 3.2°
Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2009) h = −19→27
Tmin = 0.911, Tmax = 0.963 k = −6→6
9384 measured reflections l = −14→15
2870 independent reflections