| Oxford Diffraction Xcalibur single crystal X-ray diffractometer with Sapphire CCD detector | 2178 reflections with I > 2σ(I) |
| Radiation source: Enhance (Mo) X-ray Source | Rint = 0.021 |
| Rotation method data acquisition using ω scans. | θmax = 25.4°, θmin = 3.2° |
| Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2009) | h = −19→27 |
| Tmin = 0.911, Tmax = 0.963 | k = −6→6 |
| 9384 measured reflections | l = −14→15 |
| 2870 independent reflections |