| Crystal data |
| Chemical formula |
[Pd2(C2H8N2)2(CH2O6P2)]·4H2O |
|
M
r
|
577.04 |
| Crystal system, space group |
Orthorhombic, F
d
d
d
|
| Temperature (K) |
294 |
|
a, b, c (Å) |
11.8871 (6), 12.5405 (6), 48.052 (2) |
|
V (Å3) |
7163.2 (6) |
|
Z
|
16 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
2.24 |
| Crystal size (mm) |
0.6 × 0.4 × 0.2 |
| |
| Data collection |
| Diffractometer |
Rigaku Oxford Diffraction Xcalibur, Sapphire3 |
| Absorption correction |
Multi-scan (CrysAlis PRO; Rigaku OD, 2018 ▸) |
|
T
min, T
max
|
0.418, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
14597, 2065, 1746 |
|
R
int
|
0.075 |
| (sin θ/λ)max (Å−1) |
0.649 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.063, 0.175, 1.14 |
| No. of reflections |
2065 |
| No. of parameters |
126 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.69, −2.06 |
