| Bruker Kappa APEXII CCD diffractometer | 2526 independent reflections |
| Radiation source: fine focus sealed tube | 1777 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.030 |
| φ and ω scans | θmax = 25.5°, θmin = 2.6° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 2008a) | h = −9→9 |
| Tmin = 0.955, Tmax = 0.988 | k = −9→9 |
| 12818 measured reflections | l = −13→13 |
Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.