Table 3. Experimental details.
| Crystal data | |
| Chemical formula | [Pt(C2H8N2)2][PtI2(C2H8N2)2](HSO4)4·2H2O |
| M r | 1308.70 |
| Crystal system, space group | Monoclinic, P2/n |
| Temperature (K) | 296 |
| a, b, c (Å) | 7.2964 (2), 5.9451 (2), 18.2253 (7) |
| β (°) | 92.318 (1) |
| V (Å3) | 789.93 (5) |
| Z | 1 |
| Radiation type | Mo Kα |
| μ (mm−1) | 11.15 |
| Crystal size (mm) | 0.50 × 0.40 × 0.35 |
| Data collection | |
| Diffractometer | Rigaku R-AXIS RAPID imaging plate |
| Absorption correction | Multi-scan (ABSCOR; Rigaku, 1995 ▸) |
| T min, T max | 0.010, 0.020 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 16218, 2733, 2541 |
| R int | 0.048 |
| (sin θ/λ)max (Å−1) | 0.746 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.024, 0.046, 1.21 |
| No. of reflections | 2733 |
| No. of parameters | 106 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 2.12, −1.69 |