Table 3.
Statistics for five X-ray data sets collected from single crystals of Jak1–IFN-λR1. All data were processed with HKL3000 using the common resolution ranges, 50–2.1Å and the same overall protocol.
| Set | Unit cell | #refl. tot. Red (HiRes) Compl. (HiRes) |
I/σ(I) (HiRes) Rscale (HiRes) Rpim (HiRes) |
Data for resolution 2.55 Å (data for resolution 2.73 Å) |
Data from ANSO server (UCLA) https://services.mbi.ucla.edu/anisoscale/ |
|||||
|---|---|---|---|---|---|---|---|---|---|---|
| Compl [%] | I/σ(I) | Rscale | #refl. tot | Resolution along direction | ||||||
| a* | b* | c* | ||||||||
| m5p10 | a = 165.70 b = 53.82 c = 87.40 β = 114.72 |
28,810 3.2 (2.6) 82.7 (41.2) |
18.1 (1.72) 0.058 (0.468) 0.036 (0.324) |
90.9 (98.9) |
4.78 (8.41) |
0.189 (0.154) |
28,379 | 2.1 | 2.7 | 2.1 |
| m5p11 | a = 165.53 b = 53.23 c = 87.31 β = 114.66 |
24,638 3.3 (2.2) 75.3 (18.7) |
15.2 (1.30) 0.068 (0.481) 0.041 (0.339) |
74.9 (87.3) |
3.57 (5.07) |
0.245 (0.194) |
24,157 | 2.1 | 3.3 | 2.1 |
| n2p4 | a = 166.25 b = 54.26 c = 87.43 β = 114.72 |
24,732 2.9 (1.6) 84.8 (52.6) |
13.2 (0.77) 0.078 (0.873) 0.050 (0.724) |
92.3 (97.7) |
3.60 (5.23) |
0.390 (0.286) |
24,732 | 2.2 | 2.8 | 2.1 |
| n2p6 | a = 166.58 b = 54.30 c = 87.72 β = 114.77 |
25,896 3.4 (2.6) 80.0 (43.3) |
14.7 (1.33) 0.076 (0.656) 0.048 (0.451) |
83.8 (97.1) |
3.95 (5.05) |
0.296 (0.224) |
25,650 | 2.1 | 3.1 | 2.1 |
| n2p8 | a = 166.27 b = 53.66 c = 87.40 β = 114.70 |
27,981 3.2 (2.4) 85.9 (54.1) |
18.7 (2.31) 0.054 (0.394) 0.035 (0.296) |
95.2 (99.7) |
5.29 (7.82) |
0.234 (0.177) |
27,378 | 2.1 | 2.8 | 2.1 |
| merged | a = 165.70 b = 53.80 c = 87.39 β = 114.72 |
40,748 9.4 (8.0) 98.6 (89.7) |
27.4 (1.94) 0.077 (0.634) 0.025 (0.218) |
100 (100) |
10.2 (13.4) |
0.229 (0.165) |
31,136 | 2.1 | 2.8 | 2.1 |