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. 2018 Sep 24;9(47):8883–8889. doi: 10.1039/c8sc03267j

Table 1. Polymerization conditions, bound phenolate concentrations, and TFN : CD ratio in polymer samples a .

Polymer [Phenolate] (mmol g–1) K2CO3 addition rate [TFN]0 (M) TFN : CD ratio S BET (m2 g–1) Yield (%)
TFN-CDP-2 0.44 (+/– 0.01) At once 0.3 5.2 346 (+/– 113) 64
TFN-CDP-3 0.22 (+/– 0.02) 0.1 equiv. per h 0.3 5.9 Non-porous 67
TFN-CDP-4 0.14 (+/– <0.01) At once 1.2 5.2 Non-porous 54
TFN-CDP-5 0.08 (+/– <0.01) 0.1 equiv. per h 1.2 5.9 Non-porous 54

aTFN-CDP refers to tetrafluoroterephthalonitrile-linked β-cyclodextrin polymer.