Table 1. X-ray data reduction statistics for the RGS7-Gβ5 dimer.
Isotropic scaling | |
---|---|
Space group | P 21 |
Unit cell dimensions | |
a, b, c, β | 68.32 Å, 162.76 Å, 95.29 Å, 98.36° |
Resolution (last shell) | 94.28 Å - 2.81 Å (2.86 Å - 2.81 Å) |
Total measurements | 191,664 |
No. of unique reflections (last shell) | 50,669 (2,501) |
Wavelength | 1.0 Å |
Rp.i.m.* (last shell) | 0.036 (0.431) |
I/σ(I) (last shell) | 15.1 (2.3) |
Completeness (last shell) | 0.997 (1.0) |
Multiplicity (last shell) | 3.8 (3.9) |
CC1/2 † (last shell) | 0.999 (0.868) |
Anisotropic scaling | |
Resolution (last shell) | 4.28 Å - 2.13 Å (2.48 Å - 2.13 Å) |
Total measurements | 20,4124 |
No. of unique reflections (last shell) | 54,345 (2,718) |
Wavelength | 1.0 Å |
Rp.i.m.* (last shell) | 0.038 (0.5) |
I/σ(I) (last shell) | 14.6 (2.1) |
Completeness (spherical) (last shell) | 0.47 (0.064) |
Completeness (ellipsoidal) (last shell) | 0.92 (0.63) |
Multiplicity (last shell) | 3.8 (3.7) |
CC1/2 † (last shell) | 0.999 (0.546) |
*Precision-indicating merging R factor (Weiss and Hilgenfeld, 1997; Weiss, 2001).
†Pearson correlation coefficient calculated between the average intensities of each random half of measurements of unique reflections (Karplus and Diederichs, 2012).