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. Author manuscript; available in PMC: 2019 Jun 14.
Published in final edited form as: Chem Commun (Camb). 2018 Jun 14;54(49):6296–6299. doi: 10.1039/c8cc01300d

Table 1.

Synthetic ODNs and polypeptides prepared for the conjugation studies. G* = DHP-dG, C* = 5-formyl-dC, K* = oxy-Lys.a

Sequences m/z
Calc.		 m/z Obs.
Pep-1 NH2-K*GG A 333.3 334.2
Pep-2 NH2-GGK GLG K*GG A 802.9 803.6
Pep-3 NH2-GGG KGL GKG GA 857.9 858.4
Pep-4 NH2-GGG KGL GK*G GA 859.7 860.4
DNA-1 5'-d(ATG GCG TGC* TAT)-3’ 3704.4 3704.0
DNA-2 5' -d(AG3T4C3AG*TCACGACGTT)-3' 7102.6 7103.4
DNA-3 5'-d(ATG GCG TGC TAT)-3' 3676.4 3675.6
DNA-4 5'-d(AG3T4C3AGTCACGACG TT)-3' 7030.6 7029.1
DPC-1 graphic file with name nihms-972645-t0012.jpg 4019.5 4019.1
DPC-2 graphic file with name nihms-972645-t0013.jpg 4490.5 4489.0
DPC-3 graphic file with name nihms-972645-t0014.jpg 4547.3 4546.2
DPC-4 graphic file with name nihms-972645-t0015.jpg 7387.9 7386.7
DPC-5 graphic file with name nihms-972645-t0016.jpg 7856.9 7853.2
DPC-6 graphic file with name nihms-972645-t0017.jpg 7914.5 7913.0
a

Peptides 1-4 were measured in +ve and DNA and DPCs are in −ve mode.