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. Author manuscript; available in PMC: 2019 Mar 26.
Published in final edited form as: J Am Chem Soc. 2018 Sep 17;140(38):12263–12269. doi: 10.1021/jacs.8b07865

Figure 3.

Figure 3.

(a) 500 MHz 1H NMR titrations of samples containing (a) a 1:1 mixture of Q8:peptide, (b) a 0.5:1 mixture of Q8:peptide, and (c) peptide. Spectra were acquired at 25 °C in D2O. (b) 500 MHz 2D ROESY spectra of samples containing (a) a 1:1 mixture of Q8:MYA and (b) a 1:1 mixture of Q8:MLA. The regions of the spectra displayed here reveal NOE crosspeaks between protons on neighboring side chains. Spectra were acquired at 25 °C in D2O solution.