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. Author manuscript; available in PMC: 2019 Jan 9.
Published in final edited form as: J Chromatogr B Analyt Technol Biomed Life Sci. 2018 May 16;1090:22–35. doi: 10.1016/j.jchromb.2018.05.008

Table 2.

Accuracy and precision of sera DHT, α-diol, and β-diol calibrators over five validation batches.

[XN] (ng/ml) DHT α-diol β-diol
[X¯] ± SD (ng/ml) CV (%) RE (%) [X¯] ± SD (ng/ml) CV (%) RE (%) [X¯] ± SD (ng/ml) CV (%) RE (%)
0.0500 0.051 ± 0.003 6 2 0.052 ± 0.002 4 4 0.051 ± 0.002 4 2
0.100 0.099 ± 0.007 7 −1 0.105 ± 0.008 8 5 0.095 ± 0.005 5 −5
0.250 0.23 ± 0.02 9 −8 0.26 ± 0.02 8 4 0.26 ± 0.02 8 4
0.500 0.53 ± 0.03 6 6 0.52 ± 0.02 4 4 0.51 ± 0.04 8 2
1.00 0.96 ± 0.06 6 −4 1.05 ± 0.06 6 5 0.96 ± 0.07 7 −4
5.00 5.0 ± 0.1 2 0 5.3 ± 0.3 6 6 5.2 ± 0.3 6 4
10.0 9.9 ± 0.1 1 −1 10.4 ± 0.3 3 4 9.6 ± 0.4 4 −4
50.0 48 ± 1 2 −4 52 ± 3 6 4 54 ± 1 2 8