Table 2.
no. | 1 | 2 | 3 | 4 | 5 | 6 |
---|---|---|---|---|---|---|
1 | 150.9, C | 36.6, CH | 36.5, CH2 | 206.1, C | 194.1, C | 204.9, C |
2 | 131.1, C | 50.1, CH | 142.4, C | 136.3, C | 139.4, C | 136.6, C |
3 | 124.1, CH | 82.0, C | 36.9, CH | 169.3, C | 166.3, C | 166.7, C |
4 | 120.3, CH | 39.0, CH2 | 31.0, CH2 | 81.0, C | 78.7, C | 81.5, C |
5 | 131.0, CH | 25.1, CH2 | 33.3, CH2 | 59.7, CH | 148.8, C | 58.9, CH |
6 | 111.1, CH | 40.7, CH | 71.5, CH | 59.4, CH2 | 114.7, CH2 | 24.3, CH2 |
7 | 84.1, C | 143.1, C | 136.7, C | 36.2, CH2 | 37.0, CH2 | 30.9, CH2 |
8 | 33.9, CH2 | 119.9, CH | 122.8, CH | 25.1, CH2 | 24.1, CH2 | 23.0, CH2 |
9 | 49.8, CH2 | 89.0, C | 129.3, C | 32.0, CH2 | 31.9, CH2 | 13.9, CH3 |
10 | 78.4, CH | 153.5, CH | 53.0, CH2 | 22.4, CH2 | 22.4, CH2 | 30.1, CH2 |
11 | 46.3, CH | 128.0, C | 29.2, C | 14.0, CH3 | 13.9, CH3 | 31.0, CH2 |
12 | 101.7, C | 174.0, C | 29.6, CH3 | 7.7, CH3 | 8.2, CH3 | 173.1, C |
13 | 142.6, CH | 10.4, CH3 | 29.6, CH3 | 11.3, CH3 | 10.7, CH3 | 8.0, CH3 |
14 | 21.7, CH3 | 20.2, CH3 | 17.2, CH3 | 11.3, CH3 | ||
15 | 167.4, C | 23.8, CH3 | 22.7, CH3 | |||
1′ | 146.4, C | |||||
2′ | 116.8, C | |||||
3′ | 115.4, CH | |||||
4′ | 147.4, C | |||||
5′ | 124.5, C | |||||
6′ | 119.7, CH | |||||
7′ | 15.6, CH3 | |||||
OEt | 14.5, CH3 | 14.2, CH3 | ||||
59.2, CH2 | 60.9, CH2 |
The assignments were based on HMQC, HMBC, and COSY spectra.