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. Author manuscript; available in PMC: 2019 Jan 10.
Published in final edited form as: J Nat Prod. 2016 Mar 24;79(4):1124–1131. doi: 10.1021/acs.jnatprod.6b00031

Table 2.

13C NMR Data for Compounds 1−6 (CDCl3, 150 MHz)a

no. 1 2 3 4 5 6
1 150.9, C 36.6, CH 36.5, CH2 206.1, C 194.1, C 204.9, C
2 131.1, C 50.1, CH 142.4, C 136.3, C 139.4, C 136.6, C
3 124.1, CH 82.0, C 36.9, CH 169.3, C 166.3, C 166.7, C
4 120.3, CH 39.0, CH2 31.0, CH2 81.0, C 78.7, C 81.5, C
5 131.0, CH 25.1, CH2 33.3, CH2 59.7, CH 148.8, C 58.9, CH
6 111.1, CH 40.7, CH 71.5, CH 59.4, CH2 114.7, CH2 24.3, CH2
7 84.1, C 143.1, C 136.7, C 36.2, CH2 37.0, CH2 30.9, CH2
8 33.9, CH2 119.9, CH 122.8, CH 25.1, CH2 24.1, CH2 23.0, CH2
9 49.8, CH2 89.0, C 129.3, C 32.0, CH2 31.9, CH2 13.9, CH3
10 78.4, CH 153.5, CH 53.0, CH2 22.4, CH2 22.4, CH2 30.1, CH2
11 46.3, CH 128.0, C 29.2, C 14.0, CH3 13.9, CH3 31.0, CH2
12 101.7, C 174.0, C 29.6, CH3 7.7, CH3 8.2, CH3 173.1, C
13 142.6, CH 10.4, CH3 29.6, CH3 11.3, CH3 10.7, CH3 8.0, CH3
14 21.7, CH3 20.2, CH3 17.2, CH3 11.3, CH3
15 167.4, C 23.8, CH3 22.7, CH3
1′ 146.4, C
2′ 116.8, C
3′ 115.4, CH
4′ 147.4, C
5′ 124.5, C
6′ 119.7, CH
7′ 15.6, CH3
OEt 14.5, CH3 14.2, CH3
59.2, CH2 60.9, CH2
a

The assignments were based on HMQC, HMBC, and COSY spectra.