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. Author manuscript; available in PMC: 2019 Sep 26.
Published in final edited form as: J Am Chem Soc. 2018 Sep 18;140(38):12056–12068. doi: 10.1021/jacs.8b06458

Figure 4.

Figure 4.

Different excess experiments with NFTPB. An induction period is observed at 20 mol % loading, but the rate is parallel to the standard conditions (a line has been added as a visual aid). Higher loadings of oxidant led to deleterious effects on the yield and rate, possibly due to off-pathway reactions with the nickel catalyst.