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. 2015 Sep 18;20(9):17221–17243. doi: 10.3390/molecules200917221

Table 5.

Data of the LC-TOF-MS analysis of moss ethanol extracts.

No. Formula PC RT AP CD DP HS PCC PJ PS SF SM SR ST
v1 Atraric acid 3.0 27.3 14.6 44.8 5.9 4.4 14.9 23.8 74.3 2.0 4.3 5.3 7.9
v2 Benzyl benzoate 1.6 3.4 4.1 4.2 ND 6.9 5.4 8.8 12.6 7.5 13.2 ND 5.1
v3 4-Hydroxybenzoic acid 5.6 17.7 10.1 16.2 11.2 10.1 0.8 ND 9.4 7.4 11.5 11.8 4.7
v4 Methyl 4-hydroxybenzoate 2.5 2.8 7.6 8.8 4.1 6.5 0.5 10.1 7.7 1.5 18.9 2.3 7.2
v5 3-Methoxy-4-hydroxybenzoic acid 7.7 12.5 7.9 13.5 1.2 18.2 0.7 15.4 14.5 18.2 26.6 12.1 13.4
v6 4-O-Caffeoylquinic acid ND ND ND 25.7 ND 5.0 ND ND 5.3 7.9 1.9 15.3 11.6
v7 5-O-Caffeoylquinic acid ND ND ND 25.7 ND 5.0 ND ND 5.3 7.9 1.9 15.3 11.6
v8 Caffeic acid 6.4 3.2 41.8 2.3 ND 4.0 5.8 2.9 4.4 ND ND 2.1 ND
v9 p-Coumaric acid 22.3 6.7 11.4 5.9 1.0 3.5 0.2 12.9 11.2 3.5 7.3 11.5 5.0
v10 Ferulic acid 0.8 2.7 21.3 3.3 1.2 1.1 19.1 2.7 3.0 3.7 5.6 1.5 3.9
v11 7,8-Dihydroxy-5-methoxycoumarin-7-β-sophoroside 63.2 144.1 37.1 25.0 58.0 164.9 95.9 117.3 163.8 65.7 32.8 105.3 106.5
v12 5,6,7,8-Tetrahydroxycoumarin-5-β-glucopyranoside ND ND ND ND ND ND ND ND 2.6 ND ND ND ND
v13 Abscisic acid 4.3 5.2 ND 3.9 0.7 5.3 3.9 5.9 6.5 3.7 12.5 2.9 7.3
v14 Sphagnic acid 3.4 5.5 10.0 6.4 3.6 4.4 20.3 4.4 2.1 21.9 109.0 19.0 21.8
v15 5,8-Dihydroxy-7-methoxycoumarin 5-β-glucopyranoside 35.8 1.0 7.2 6.1 12.8 4.3 4.5 4.1 2.6 9.8 6.6 30.6 10.5
v16 Dimethyl phthalate 0.8 2.7 21.3 3.3 1.2 1.1 19.1 2.7 3.0 3.7 5.7 1.5 3.9
v17 Dimethyl terephthalate 0.8 2.7 21.3 3.3 1.2 1.1 19.1 2.7 3.0 3.7 5.7 1.5 3.9
v18 Ohioensin H 208.8 ND 0.8 6.1 5.3 4.1 6.6 5.6 2.5 10.3 11.7 7.4 7.6
V19 Harmol propionic acid ester ND ND ND ND ND ND ND ND ND ND ND 0.6 ND
v20 7-Hydroxyharmane ND ND ND ND ND ND ND ND ND ND ND 0.6 ND
v21 Apigenin ND 69.0 69.5 71.6 6.0 36.4 ND ND 21.7 ND 5.8 ND ND
v22 2,3-Dihydro-5ʹ,3ʹʹʹ-dihydroxyamentoflavone 6.1 25.0 24.7 47.4 ND 9.3 ND 78.8 3.3 ND ND ND ND
v23 2,3-Dihydrodicranolomin 6.1 25.0 24.7 47.4 ND 9.3 ND 78.8 3.3 ND ND ND ND
v24 Communin A 20.5 ND ND 3.5 ND ND ND ND 2.2 ND 1.4 ND ND
v25 2,3-Dihydro-5ʹ-hydroxyrobustaflavone ND 0.8 ND ND ND ND 3.7 ND ND ND ND ND 1.3
v26 3ʹʹʹ-Desoxydicranolomin ND 114.8 102.7 ND ND 14.7 ND ND 17.3 ND 0.7 ND ND
v27 3-Hydroxy-β-ionone 4.9 62.0 91.0 9.7 5.8 66.3 7.7 14.6 21.9 2.1 36.6 5.9 14.5
v28 p-Hydroxyacetophenone 1.2 31.2 32.3 16.3 0.0 18.4 12.0 ND 6.2 344.4 63.1 25.2 67.7
V29 3,5-dioxohexanoic acid 179.9 98.3 99.3 43.7 99.0 97.6 162.7 91.4 118.3 64.2 70.4 76.5 103.9
V30 4-hydroxybenzoic acid 5.5 17.7 10.1 17.3 11.2 10.1 0.8 ND 9.4 7.4 11.5 11.8 4.7
v31 Α-d-furanallulose ND ND ND ND ND ND 6.3 ND 1.3 0.8 1.6 1.0 ND
v32 Benzoic acid 11.8 5.1 0.0 5.2 ND 8.9 4.1 8.8 15.0 4.9 4.8 11.0 13.1
v33 Protocatechuic acid 6.3 11.3 18.4 18.5 5.2 15.9 12.2 10.6 9.5 8.2 13.0 8.7 10.9
v34 Vanillic acid 6.8 12.5 8.2 13.7 4.2 18.2 10.1 15.4 14.5 11.4 13.6 9.0 13.4
v35 Matairesinol ND ND ND 4.4 0.4 ND ND ND ND ND ND ND ND
v36 Glycine 7.8 31.2 18.4 20.6 16.2 35.3 31.0 20.5 14.1 12.4 19.0 19.2 23.3
v37 Alanine 200.5 145.4 166.0 84.4 297.0 82.6 154.8 60.0 94.4 78.1 407.8 139.8 137.2
v38 Serine 42.1 77.2 57.4 43.8 72.2 112.5 176.1 144.5 178.6 27.4 46.0 27.1 89.7
V39 Glutamic acid 69.8 765.3 709.9 262.5 75.7 1039.5 890.0 846.4 1134.6 135.6 77.7 10.8 587.8
v40 Proline 21.5 95.0 55.6 105.8 24.6 99.6 61.8 37.2 42.3 17.9 46.6 25.3 73.4
v41 Valine 397.6 253.7 208.4 188.9 290.0 255.1 373.5 443.5 188.6 84.3 176.2 53.4 298.9
v42 Threonine 51.4 51.8 62.3 27.7 43.2 81.7 105.7 72.9 73.0 26.1 98.0 12.1 99.0
v43 Leucine 54.5 45.0 278.4 74.9 47.4 57.2 81.0 68.7 121.0 55.3 448.3 15.1 176.0
v44 Asparagine 147.6 ND ND ND ND ND 541.1 0.0 ND ND 589.6 0.9 ND
v45 Aspartic acid 194.0 269.0 276.6 42.3 52.4 419.9 507.9 216.8 427.3 49.1 67.5 15.9 186.7
v46 Glutamine 29.9 9.4 8.3 4.9 5.4 5.6 6.1 17.7 7.2 ND 9.8 ND 1.6
v47 Lysine 3.3 0.8 30.5 30.5 2.7 4.4 5.5 1.2 2.6 0.5 6.2 9.1 3.1
v48 Phenylalanine 103.4 69.1 519.1 124.6 32.6 108.6 171.7 45.4 89.9 22.5 355.7 13.3 56.3
V49 Arginine 5.1 30.4 15.5 11.5 3.7 53.6 25.4 84.3 107.0 59.1 95.9 4.0 9.7
v50 Tyrosine 36.2 2.4 25.1 6.4 13.3 21.2 26.7 16.4 13.3 3.3 15.9 3.6 8.6
v51 Tryptophan 75.4 20.7 378.7 159.6 11.6 35.6 107.4 45.9 42.4 18.5 161.1 27.2 38.3

ND, not detected.