Table 2.
Position | δC, Type | δC (J in Hz) | HMBC |
---|---|---|---|
1 | 126.4, CH | 8.58, s | C-3, 4a, 9, 11 |
2 | 135.9, C | - | |
3 | 132.7, C | - | |
4 | 133.5, C | - | |
4a | 152.5, C | - | |
5 | 102.9, CH | 6.93, s | C-7, 8a, 9, 10a |
6 | 150.7, C | - | |
7 | 144.6, C | - | |
8 | 108.6, CH | 7.48, s | C-7, 8a, 9, 10a |
8a | 115.7, C | - | |
9 | 173.4, CO | - | |
9a | 119.8, C | ||
10a | 154.5, C | ||
11 | 199.2, CO | ||
12 | 29.2, CH3 | 2.55, s | C-2, 11 |
13 | 201.3, CO | - | |
14 | 32.3, CH3 | 2.53, s | C-4, 13 |
2′ | 152.9, CH | 8.13, s | C-3′, 4′, 8′a, 9′ |
3′ | 120.8, C | - | |
4′ | 173.7, CO | - | |
4′a | 113.4, C | - | |
5′ | 107.9, CH | 7.28, brs | C-4’, 6′, 7′, 8′a |
6′ | 152.8, C | - | |
7′ | 145.0, C | - | |
8′ | 103.1, CH | 6.94, s | C-4′, 6′, 7′ |
8′a | 151.1, C |