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. 2019 Jan 8;24(1):208. doi: 10.3390/molecules24010208

Table 2.

The 1H- and 13C-NMR (DMSO-d6, 500 and 125 MHz) and HMBC assignment for 2.

Position δC, Type δC (J in Hz) HMBC
1 126.4, CH 8.58, s C-3, 4a, 9, 11
2 135.9, C -
3 132.7, C -
4 133.5, C -
4a 152.5, C -
5 102.9, CH 6.93, s C-7, 8a, 9, 10a
6 150.7, C -
7 144.6, C -
8 108.6, CH 7.48, s C-7, 8a, 9, 10a
8a 115.7, C -
9 173.4, CO -
9a 119.8, C
10a 154.5, C
11 199.2, CO
12 29.2, CH3 2.55, s C-2, 11
13 201.3, CO -
14 32.3, CH3 2.53, s C-4, 13
2′ 152.9, CH 8.13, s C-3′, 4′, 8′a, 9′
3′ 120.8, C -
4′ 173.7, CO -
4′a 113.4, C -
5′ 107.9, CH 7.28, brs C-4’, 6′, 7′, 8′a
6′ 152.8, C -
7′ 145.0, C -
8′ 103.1, CH 6.94, s C-4′, 6′, 7′
8′a 151.1, C