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. Author manuscript; available in PMC: 2019 Jan 18.
Published in final edited form as: Food Chem. 2014 Oct 13;173:231–237. doi: 10.1016/j.foodchem.2014.09.170

Table 2.

13C NMR (100 MHz, CDCl3) data for compounds 1–5.

Positions 1 2 3 4 5

1 134.0 s 130.0 s 131.0 s 131.8 s 130.6 s
2 106.7 d 110.4 d 102.9 d 104.1 d 102.7 d
3 147.5 s 148.8 s 146.8 s 146.9 s 146.9 s
4 146.4 s 148.7 s 133.8 s 134.3 s 133.8 s
5 107.9 d 110.8 d 146.8 s 146.9 s 146.9 s
6 119.1 d 119.6 d 102.9 d 104.1 d 102.7 d
7 72.9 d 77.2 d 73.7 d 79.4 d 73.4 d
8 82.4 d 80.4 d 82.2 d 86.6 d 83.1 d
9 12.7 q 14.8 q 13.3 q 17.6 q 12.7 q
1′ 133.8 s 138.6 s 145.5 s 135.3 s 137.8 s
2′ 153.6 s 153.8 s 151.3 s 152.7 s 154.0 s
3′ 102.9 d 105.7 d 109.2 d 105.5 d 105.6 d
4′ 134.1 s 129.5 s 133.5 s 135.9 s 129.9 s
5′ 102.9 d 105.7 d 118.9 d 105.5 d 105.6 d
6′ 153.6 s 153.8 s 119.5 d 152.7 s 154.0 s
7′ 130.8 d 152.7 d 130.4 d 40.2 t 152.3 d
8′ 125.7 d 127.9 d 124.9 d 137.0 d 128.2 d
9′ 18.4 q 193.4 d 18.3 q 116.2 t 193.3 d
OCH2O 100.8 t
COCH3 170.1 s
21.2 q
2′-OMe 56.1 q 56.1 q 55.7 q 56.0 q 56.33 q
6′-OMe 56.1 q 56.1 q 56.0 q 56.33 q
3-OMe 55.91 q 56.2 q 56.3 q 56.29 q
4-OMe 55.89 q
5-OMe 56.2 q 56.3 q 56.29 q

C-multiplicities were established by a HSQC experiment. s: C; d: CH; t: CH2; q: CH3.