Table 2.
Positions | 1 | 2 | 3 | 4 | 5 |
---|---|---|---|---|---|
1 | 134.0 s | 130.0 s | 131.0 s | 131.8 s | 130.6 s |
2 | 106.7 d | 110.4 d | 102.9 d | 104.1 d | 102.7 d |
3 | 147.5 s | 148.8 s | 146.8 s | 146.9 s | 146.9 s |
4 | 146.4 s | 148.7 s | 133.8 s | 134.3 s | 133.8 s |
5 | 107.9 d | 110.8 d | 146.8 s | 146.9 s | 146.9 s |
6 | 119.1 d | 119.6 d | 102.9 d | 104.1 d | 102.7 d |
7 | 72.9 d | 77.2 d | 73.7 d | 79.4 d | 73.4 d |
8 | 82.4 d | 80.4 d | 82.2 d | 86.6 d | 83.1 d |
9 | 12.7 q | 14.8 q | 13.3 q | 17.6 q | 12.7 q |
1′ | 133.8 s | 138.6 s | 145.5 s | 135.3 s | 137.8 s |
2′ | 153.6 s | 153.8 s | 151.3 s | 152.7 s | 154.0 s |
3′ | 102.9 d | 105.7 d | 109.2 d | 105.5 d | 105.6 d |
4′ | 134.1 s | 129.5 s | 133.5 s | 135.9 s | 129.9 s |
5′ | 102.9 d | 105.7 d | 118.9 d | 105.5 d | 105.6 d |
6′ | 153.6 s | 153.8 s | 119.5 d | 152.7 s | 154.0 s |
7′ | 130.8 d | 152.7 d | 130.4 d | 40.2 t | 152.3 d |
8′ | 125.7 d | 127.9 d | 124.9 d | 137.0 d | 128.2 d |
9′ | 18.4 q | 193.4 d | 18.3 q | 116.2 t | 193.3 d |
OCH2O | 100.8 t | ||||
COCH3 | 170.1 s | ||||
21.2 q | |||||
2′-OMe | 56.1 q | 56.1 q | 55.7 q | 56.0 q | 56.33 q |
6′-OMe | 56.1 q | 56.1 q | 56.0 q | 56.33 q | |
3-OMe | 55.91 q | 56.2 q | 56.3 q | 56.29 q | |
4-OMe | 55.89 q | ||||
5-OMe | 56.2 q | 56.3 q | 56.29 q |
C-multiplicities were established by a HSQC experiment. s: C; d: CH; t: CH2; q: CH3.