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. Author manuscript; available in PMC: 2019 Jan 18.
Published in final edited form as: J Chromatogr B Analyt Technol Biomed Life Sci. 2016 Dec 21;1041-1042:104–112. doi: 10.1016/j.jchromb.2016.12.026

Table 2.

Inter/intra-day accuracy and precision for each component in serum after oral administration of Xian-ling-gu-bao extracts.

Compounds Conc. (ng/mL) Intra-day (n = 6)
Inter-day (n = 18)
Measured conc. (ng/mL) RE% RSD% Measured conc. (ng/mL) RE% RSD%
Sweroside 50 50.9 ± 5.1 5.1 10.0 51.3 ± 1.0 2.7 2.0
200 203.1 ± 25.1 3.8 12.3 204.1 ± 3.1 2.1 1.5
1600 1617.3 ± 143.0 −10.1 8.8 1524.2 ± 89.5 −4.7 5.9
Magnoflorine 3 3.0 ± 0.3 6.8 8.3 3.1 ± 0.1 4.6 2.9
150 155.1 ± 10.9 8.1 7.0 159.2 ± 3.7 6.2 2.3
1200 1090.8 ± 35.8 −11.0 3.3 1077.7 ± 11.6 −10.2 1.1
Epimedin C 5 5.1 ± 0.5 −2.6 9.1 5.0 ± 0.1 0.7 2.9
200 212.1 ± 13.5 10.8 6.4 217.0 ± 4.7 8.5 2.2
1600 1486.2 ± 55.4 −11.6 3.7 1451.7 ± 36.0 −9.3 2.5
Akebia saponin D 50 50.3 ± 5.2 8.4 10.3 52.6 ± 2.0 5.2 3.9
200 215.2 ± 19.2 11.0 8.9 216.0 ± 5.6 8.0 2.6
1600 1460.9 ± 71.5 −11.0 4.9 1427.9 ± 31.7 −10.8 2.2
Psoralen 10 10.1 ± 1.0 −6.0 10.0 9.9 ± 0.4 −1.4 4.0
300 289.4 ± 13.5 5.2 4.6 304.4 ± 13.5 1.5 4.4
2400 2507.9 ± 185.9 −10.7 7.4 2343.1 ± 184.5 −2.4 7.9
Isopsoralen 10 10.5 ± 1.1 4.3 10.4 10.0 ± 0.4 −0.2 4.1
150 145.4 ± 12.5 −3.1 8.6 150.2 ± 4.2 0.1 2.8
1200 1172.3 ± 75.2 −9.3 6.4 1162.5 ± 69.5 −3.1 6.0
Neobavaisoflavone 1 1.0 ± 0.1 2.4 8.9 1.0 ± 0.1 1.6 1.9
30 31.4 ± 2.4 9.5 7.6 32.1 ± 0.7 7.0 2.3
240 230.3 ± 10.0 −11.9 4.3 220.7 ± 9.4 −8.1 4.2
Icariside II 1 1.1 ± 0.1 8.0 4.8 1.1 ± 0.1 7.8 0.9
20 20.8 ± 2.0 8.3 9.5 21.3 ± 0.5 6.5 2.2
160 146.5 ± 5.3 −11.2 3.6 149.7 ± 9.1 −10.2 6.1
Corylin 2.5 2.4 ± 0.3 5.6 11.4 2.5 ± 0.1 0.4 5.4
10 10.2 ± 1.1 3.2 10.7 10.2 ± 0.1 1.9 1.1
80 76.0 ± 5.2 −8.3 6.8 75.7 ± 2.1 −5.4 2.8
Psoralidin 2 2.1 ± 0.2 4.7 10.0 2.1 ± 0.1 2.4 2.5
50 55.3 ± 2.5 10.6 4.5 54.7 ± 0.5 9.5 0.9
400 360.4 ± 11.9 −12.7 3.3 354.7 ± 5.6 −11.3 1.6
Bavachinin 2 1.9 ± 0.2 −9.5 9.1 1.9 ± 0.1 −5.6 3.8
10 9.9 ± 1.0 8.7 10.2 10.4 ± 0.5 4.1 4.7
80 73.0 ± 3.6 −12.3 4.9 72.1 ± 1.7 −9.8 2.4

Conc. means concentration.