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. 2018 Dec 7;30(1):70–82. doi: 10.1021/acs.bioconjchem.8b00731

Scheme 1. Synthesis of Anomeric Mannopentaoside Azidopropyl Spacer Derivatives 2 and 4.

Scheme 1

Reagents and conditions: K2CO3, imidazole-1-sulfonyl azide·HCl, 0.1 M CuSO4·5H2O, 2:1 MeOH–H2O, rt 24 h.