Table 3.

Decomposition study

#	Off-time (min)	Yield (mg)	% dead	Mw × 10−6	Mn × 10−6	Đ
1	0	770	0	1.61	1.15	1.40
2	10	565	27	1.23	0.94	1.31
3	30	360	54	1.80	1.28	1.41
4	60	110	86	1.60	1.10	1.46

PMAO-IP polymethylaluminoxane, GPC gel permeation chromatography, M_n number average molecular weight, M_w weight average molecular weight

Standard conditions: Catalyst 6 0.5 µmol, PMAO-IP 1750 equiv., toluene 25 mL, 100 equiv. ethylene added via syringe into solution; wait X minutes, then bubble ethylene directly into the solution. The molecular weight was determined by GPC in 1,2,4-trichlorobenzene