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. 2019 Jan 14;15:130–136. doi: 10.3762/bjoc.15.13

Table 1.

Chemical shift values (ppm) of four LM5CCs with the assignmentsa.

graphic file with name Beilstein_J_Org_Chem-15-130-i001.jpg

1a 1b 1c 1d

154.6 (C11) 155.1 (C11) 155.2 (C11) 154.4 (C11)
147.2 (C7) 145.7 (C7) 146.4 (C7) 147.3 (C7)
110.0 (C8) 111.9 (C8) 110.7 (C8) 109.8 (C8)
82.0 (C1) 86.2 (C1) 85.4 (C1) 82.6 (C1)
80.4 (C2) 81.6 (C2) 84.8 (C2) 81.7 (C2)
39.8 (C4) 38.5 (C4) 43.0 (C4) 37.3 (C4)
33.9 (C3) 31.7 (C6) 33.0 (C6) 34.1 (C6)
32.9 (C6) 25.8 (C3) 28.9 (C3) 30.5 (C3)
26.1 (C10) 25.1 (C5) 27.9 (C5) 26.2 (C5)
25.6 (C5) 22.5 (C9) 20.8 (C9) 22.2 (C10)
20.5 (C9) 16.8 (C10) 16.9 (C10) 20.8 (C9)

aIn CDCl3.