Table 1.
Selected Rietveld analysis parameters.
| Sample | Ox,y,z (*) | i (*) | Micro Absorption Correction | Overall Temperature Factor, Bover | Lattice Constant (nm) |
Size (nm) | Rf | χ2 |
|---|---|---|---|---|---|---|---|---|
| MnFe2O4 | 0.251 | 0.928 | No | 0 (+) | 0.84693 | 13.8 | 9.03 | 1.33 |
| MnFe2O4 | 0.251 | 0.898 | No | −2.79 | 0.84684 | 13.2 | 4.45 | 1.18 |
| MnFe2O4 | 0.257 | 0.60 | Yes (#) | 0 (+) | 0.84685 | 13.3 | 3.18 | 1.18 |
| MnFe2O4/Au | 0.257 (+) | 0.60 (+) | Yes (##) | 0 (+) | 0.84685 (+) | 13.3 | 4.70 | 1.56 |
| --- | --- | 0 (+) | 0.406945 | 11.7 | 0.68 |
(#) P0 = 0.629, C = 1.31, τ = 0.055. (##) P0 = 0.607, C = 1.15, τ = 0.084. (+) fixed values. (*) Values in CIF file 2360018 are Ox,y,z = 0.25053 and i = 0.33.