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. 2019 Jan 15;24(2):301. doi: 10.3390/molecules24020301

Table 1.

The 1H and 13C-NMR assignments of compound 1.

Atom C Shift H Shift H Multiplicity
1 44.6 1.27 m
2.14 dd (12.7, 4.4)
2 68.0 3.58 m
3 82.4 2.82 d (9.7)
4 38.9
5 48.8 1.11 m
6 23.0 2.05 m
7 123.8 5.57 d (5.2)
8 142.2
9 149.2
10 38.8
11 117.2 5.30 br s
12 79.7 3.70 br s
13 45.3
14 47.8
15 33.0 1.74 m
1.46 m
16 25.6 1.88 m
1.49 m
17 46.2 1.44 m
18 13.9 0.50 s
19 22.3 0.97 s
20 38.2 1.75 m
21 73.8 3.91 dd (11.5, 4.3)
2.95 t (11.1)
22 29.3 1.17 m
1.30 m
23 28.6 1.54 m
1.15 m
24 78.4 3.09 dd (9.8, 1.6)
25 72.3
26 23.4 1.02 s
27 24.4 1.05 s
28 24.1 0.80 s
29 16.1 0.80 s
30 27.8 0.91 s